![]() Method of preparation of an oral ingestion preparation of mare's milk (Machine-translation by Go
专利摘要:
A method of preparing an oral ingestion preparation of lyophilized mare's milk for use as a food supplement and cosmetic product comprising a step of heat treatment by pasteurization, a step of treatment with antioxidants, a cooling step, a freezing step and a lyophilization stage. (Machine-translation by Google Translate, not legally binding) 公开号:ES2664122A1 申请号:ES201600882 申请日:2016-10-18 公开日:2018-04-18 发明作者:Francisco Salvador PARDO GARROTE 申请人:Ecoser 05 S L;Ecoser 05 SL; IPC主号:
专利说明:
Object of the invention The object of the present invention is a method of preparing an oral ingestion preparation based on freeze-dried mare's milk, in which said preparation is used as a food supplement or cosmetic treatment formulation. State of the art The milk of mare has a fat content, susceptible to oxidation at temperatures above 24 ° C and a presence of humidity greater than 60% causing its thickening, which disables it for consumption due to the deterioration of its organoleptic properties. of rooting is presented by all the preparations of mare's milk existing in the market, which causes a serious limitation due to the smell of rancid, disabling it for consumption as an oral ingestion preparation for food use and cosmetic use. Document ES 2 306 863 T3 describes the use of dried concentrated mare's milk on a biologically inert high dispersion matrix. This document refers to the use of dried mare milk dried on a matrix of high dispersion, biologically inert for the preparation of an oral ingestion preparation for the treatment of skin diseases, especially dry skin diseases. According to the description of this document, native mare's milk presents the storage problem, since it is not stable for storage at room temperature. Native mare's milk can be kept only for a few days at room temperature, refrigerated for only about a week and frozen for a maximum of half a year. Therefore, a product that gives stability to mare's milk is necessary, which in the aforementioned document is done by concentrated (durable) dried mare's milk on a biologically inert, high dispersion matrix, is especially suitable for treatment of skin diseases and, in comparison with the native milk of mare, presents a high stability during storage even at room temperature. However, this procedure is expensive and difficult to carry out, so a method of making a preparation based on mare's milk that allows its preservation and use for a long time remains a necessity. 5 Description of the invention An object of the present invention is a method of preparing an oral ingestion preparation of lyophilized mare's milk suitable for use as a food supplement and cosmetic product that is essentially characterized in that it comprises a stage of 10 heat treatment by pasteurization, an antioxidant treatment stage, a cooling stage, a freezing stage and a lyophilization stage. One of the problems solved by the present invention is the strong presence of microbes in raw mare's milk. For this, a treatment process is established 15 thermal pasteurization at low temperature (preferably 65 ° e for 5 minutes) to achieve a treatment of bifid bacteria and elimination of pathogenic bacteria. In addition, raw mare's milk is expected to have the qualification of "organic milk" according to ES-ECO-023-MA Agriculture VE control certification. Another problem facing the present invention is the conservation problems of raw mare's milk. To this end, the present invention adds antioxidant to stabilize the fats and the previously pasteurized milk is subjected to a cold chilling process, so that the milk reaches an ooe temperature as soon as possible, but without going to a solid state by freezing, avoiding lower the temperature to a point that 25 eliminates latent freezing heat. Finally, for the preservation of mare's milk, it is lyophilized. However, the milk must be conditioned so that the lyophilization process can be carried out. This conditioning stage is based on freezing in individual forms (IQF, 30 Individual Quick Freezing) of 1 Ox1 Ox1 O mm in a silicone mold, optimal volume that allows to obtain lyophilized dry extract of freeze-dried mare's milk through the lyophilization process, with conclusive improvements in product quality, minimization of consumption of energy and reduction in a logarithmic unit of the bacterial forming units, controlling the optimal microbiology for the described uses. Throughout the description and the claims the word "comprises" and its variants are not intended to exclude other technical characteristics, additives, components or steps. For those skilled in the art, other objects, advantages and features of the invention will be derived partly from the description and partly from the practice of the invention. The following examples and drawings are provided by way of illustration, and are not intended to restrict the present invention. In addition, the present invention covers all possible combinations of particular and preferred embodiments indicated herein. Example The present invention is based on obtaining a dry extract of freeze-dried mare's milk by means of a low temperature process that prevents cracking of the molecular structures of the components of the mare's milk, contributing to obtain a product of the best quality. Obtaining an oral ingestion preparation of freeze-dried mare's milk. In an example of obtaining a preparation of mare's milk, the mare has a previously selected diet, especially so that the diet is rich in vitamins and tocopherols. Subsequently, each mare is milked by vacuum and the raw mare's milk is transported to the milk collection center at an OOC temperature where macroscopic filtration of the raw mare's milk is performed. Subsequently, raw mare's milk is heat treated by pasteurization at 65 ° C for 5 minutes. Pasteurized mare's milk is treated with antioxidants, preferably vitamin E and more preferably an extract rich in tocopherols. Mare's milk, once pasteurized and treated with antioxidants, is cooled to 0 ° C, but without going to a solid state, keeping the milk in a liquid state, so that at that temperature of 0 ° C, the Milk can be poured onto a silicone mold with individual forms of 1Ox1 Ox1 Omm, establishing a rapid freezing (IQF) at -24 ° C until the temperature stabilizes. The individual forms, which are cubes of 1 Ox1 Ox1 O mm mare's milk, pass to a freeze dryer with a working temperature range of -20 ° C at room temperature. that a dry lyophilized extract of mare's milk is obtained that, finally, will be ground and encapsulated in a vegetable capsule of hypromelanose (HPMC) for its subsequent placing on the market.
权利要求:
Claims (1) [1] 1 -A method of preparing an oral ingestion preparation of freeze-dried mare's milk that is characterized in that it comprises a pasteurization heat treatment stage, an antioxidant treatment stage, a cooling stage, a freezing stage and a lyophilization stage . 2 - The method according to claim 1 wherein the heat treatment step by pasteurization is performed on raw mare's milk at 65 ° C for 5 minutes. 3. The method according to any of claims 1-2 wherein in the cooling stage, the pasteurized raw mare's milk is cooled to OOC without going to solid state. 4 - The method according to any of claims 1-3 wherein the freezing step comprises the pouring of pasteurized mare's milk at 0 ° C onto a silicone mold with individual shapes of 1 Ox1 Ox1 Omm and freezing at - 24 ° C 5. The method according to any of claims 1-4 wherein the lyophilization step from -20 ° C at room temperature and comprising obtaining freeze dried dry extract of the individual forms of frozen mare's milk. 6 - The method according to any of claims 1-5 comprising the milling and encapsulation steps of the lyophilized mare's milk. 7 - An oral ingestion preparation of mare's milk obtained by the method of any one of claims 1 to 6 comprising lyophilized mare's milk, antioxidant and a coating agent. 8 - The preparation of claim 7 wherein the antioxidant is vitamin E and preferably an extract rich in tocopherol. 9. The preparation of any one of claims 7 or 8 wherein the coating agent is a vegetable capsule of hypromelanose (HPMC). 10. Use of the preparation of any of claims 7 to 9 as a food supplement. 11 -Use of the preparation of any of claims 7 to 9 as cosmetic product.
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公开号 | 公开日 ES2664122B1|2019-01-25|
引用文献:
公开号 | 申请日 | 公开日 | 申请人 | 专利标题 AT393961B|1989-04-26|1992-01-10|Fuchs Norbert Mag|High quality dry mareÆs milk powder|
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申请号 | 申请日 | 专利标题 ES201600882A|ES2664122B1|2016-10-18|2016-10-18|Method of preparation of an oral ingestion preparation of mare's milk|ES201600882A| ES2664122B1|2016-10-18|2016-10-18|Method of preparation of an oral ingestion preparation of mare's milk| 相关专利
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